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Use of Ion Exchange To Regulate the Heterogeneous Ice Nucleation Efficiency of Mica

  • Shenglin Jin
    Shenglin Jin
    Key Laboratory of Green Printing, Beijing National Laboratory for Molecular Science, Institute of Chemistry, Chinese Academy of Sciences, Beijing 100190, China
    More by Shenglin Jin
  • , 
  • Yuan Liu
    Yuan Liu
    Beijing Advanced Innovation Center for Soft Matter Science and Engineering, Beijing University of Chemical Technology, Beijing 100029, China
    Department of Chemistry, University of Nebraska—Lincoln, Lincoln, Nebraska 68588, United States
    More by Yuan Liu
    Orcidhttp://orcid.org/0000-0002-8239-7704
  • , 
  • Malte Deiseroth
    Malte Deiseroth
    Max Planck Institute for Polymer Research, 55128 Mainz, Germany
    More by Malte Deiseroth
  • , 
  • Jie Liu
    Jie Liu
    Key Laboratory of Green Printing, Beijing National Laboratory for Molecular Science, Institute of Chemistry, Chinese Academy of Sciences, Beijing 100190, China
    More by Jie Liu
    Orcidhttp://orcid.org/0000-0002-0014-5635
  • , 
  • Ellen H. G. Backus
    Ellen H. G. Backus
    Max Planck Institute for Polymer Research, 55128 Mainz, Germany
    Department of Physical Chemistry, University of Vienna, Währinger Strasse 42, 1090 Wien, Austria
    More by Ellen H. G. Backus
    Orcidhttp://orcid.org/0000-0002-6202-0280
  • , 
  • Hui Li
    Hui Li
    Beijing Advanced Innovation Center for Soft Matter Science and Engineering, Beijing University of Chemical Technology, Beijing 100029, China
    More by Hui Li
    Orcidhttp://orcid.org/0000-0002-1725-6796
  • , 
  • Han Xue
    Han Xue
    Key Laboratory of Green Printing, Beijing National Laboratory for Molecular Science, Institute of Chemistry, Chinese Academy of Sciences, Beijing 100190, China
    More by Han Xue
  • , 
  • Lishan Zhao
    Lishan Zhao
    Key Laboratory of Green Printing, Beijing National Laboratory for Molecular Science, Institute of Chemistry, Chinese Academy of Sciences, Beijing 100190, China
    More by Lishan Zhao
  • , 
  • Xiao Cheng Zeng*
    Xiao Cheng Zeng
    Department of Chemistry, University of Nebraska—Lincoln, Lincoln, Nebraska 68588, United States
    *[email protected]
    More by Xiao Cheng Zeng
    Orcidhttp://orcid.org/0000-0003-4672-8585
  • , 
  • Mischa Bonn*
    Mischa Bonn
    Max Planck Institute for Polymer Research, 55128 Mainz, Germany
    *[email protected]
    More by Mischa Bonn
    Orcidhttp://orcid.org/0000-0001-6851-8453
  • , and 
  • Jianjun Wang*
    Jianjun Wang
    Key Laboratory of Green Printing, Beijing National Laboratory for Molecular Science, Institute of Chemistry, Chinese Academy of Sciences, Beijing 100190, China
    School of Chemistry and Chemical Engineering, University of Chinese Academy of Sciences, Beijing 100049, China
    *[email protected]
    More by Jianjun Wang
    Orcidhttp://orcid.org/0000-0002-1704-9922
Cite this: J. Am. Chem. Soc. 2020, 142, 42, 17956–17965
Publication Date (Web):September 27, 2020
https://doi.org/10.1021/jacs.0c00920
Copyright © 2020 American Chemical Society
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    Abstract

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    Heterogeneous ice nucleation (HIN) triggered by mineral surfaces typically exposed to various ions can have a significant impact on the regional atmosphere and climate. However, the dependence of HIN on the nature of the mineral surface ions is still largely unexplored due to the complexity of mineral surfaces. Because K+ on the atomically flat (001) surface of mica can be readily replaced by different cations through ion exchange, muscovite mica was selected; its simple nature provides a very straightforward system that can serve as the model for investigating the effects of mineral surface ions on HIN. Our experiments show that the surface (001) of H+-exchanged mica displays markedly higher HIN efficiencies than that of Na-/K-mica. Vibrational sum-frequency generation spectroscopy reveals that H-mica induces substantially less orientation ordering than Na-/K-mica within the contact water layer at the interface. Molecular dynamics simulations suggest that the HIN efficiency of mica depends on the positional arrangement and orientation of the interfacial water. The formation of the hexagonal ice Ih basal-type structure in the first water layer atop the mica surface facilitates HIN, which is determined by the size of the protruding ions atop the mica surface and by the surface adsorption energy. The orientational distribution is optimal for HIN when 25% of the water molecules in the first water layer atop the mica surface have one OH group pointing up and 25% have one OH group pointing down, which, in turn, is determined by the surface charge distribution.

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