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Deposition of Carboxymethylcellulose-Coated Zero-Valent Iron Nanoparticles onto Silica: Roles of Solution Chemistry and Organic Molecules

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† Department of Chemical Engineering, McGill University, Montreal, Quebec H3A 2B2, Canada
‡ Department of Civil Engineering, McGill University, Montreal, Quebec H3A 2K6, Canada
*Corresponding author. Phone: (514) 398-2999. Fax: (514) 398-6678. E-mail: [email protected]
Cite this: Langmuir 2010, 26, 15, 12832–12840
Publication Date (Web):July 1, 2010
https://doi.org/10.1021/la1006633
Copyright © 2010 American Chemical Society
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    Abstract

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    Zero-valent iron nanoparticles (nZVI) used in the remediation of contaminated subsurface environments are commonly stabilized using polymer coatings. A bottom-up synthesis approach was used to synthesize carboxymethylcellulose (CMC)-coated nZVI particles with increased colloidal stability. The influence of water chemistry and selected environmental molecules, namely, fulvic acids and rhamnolipids, on the aggregate size and surface charge of the bare and CMC-coated nZVI particles was systematically examined using dynamic light scattering (DLS), nanoparticle tracking analysis (NTA), and laser Doppler velocimetry. A quartz crystal microbalance with energy dissipation monitoring (QCM-D) was used to quantify the deposition rates of bare and CMC-coated nZVI particles onto a silica surface over a broad range of solution ionic strengths and in the presence of naturally occurring molecules. Nanoscale ZVI particle deposition was found to increase with IS for many of the conditions investigated. CMC acted as a better colloidal stabilizer when covalently bound to nZVI particles than when physisorbed onto the nanoparticle surface after particle synthesis. The lowest nanoparticle deposition rates were observed for CMC-coated nZVI in the presence of the rhamnolipid biosurfactant.

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    Representative TEM micrographs of bare and CMC-nZVI particles obtained from drying drops of salt-free suspensions. Values of the energy barrier maxima and secondary energy minima for bare and CMC-coated nZVI particles, determined from calculated DLVO interaction energy profiles for simple electrolyte conditions. Values of the energy barrier maxima and secondary energy minima for bare and CMC-coated nZVI particles, determined from calculated DLVO interaction energy profiles in the presence of 2 mg/L fulvic acid or 2 mg/L rhamnolipid. This material is available free of charge via the Internet at http://pubs.acs.org.

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