Abstract
The timing of Palaeolithic human activities in South China is still controversial because of the lack of a reliable chronology of archaeological sites. The Longdengshan Palaeolithic site (LPS), located close to the Wuyi Mountain of South China, represents the first discovered and scientifically excavated Middle Palaeolithic site in the Fujian Province. This site is of considerable significance for studying the diffusion and cultural connotation of early Homo sapiens in southern China. In this study, we present optically stimulated luminescence (OSL) ages obtained from medium-grained quartz collected at the LPS. The single-aliquot regenerative-dose measurements of red soil deposits collected at the same site yielded internally and stratigraphically consistent ages and similar errors, indicating a potential ability of the technique, and also reflecting the influence of various sedimentary facies on the test results. Our results indicate that the 38–63 µm quartz grains were generally partially-bleached and had large values of over-dispersion in the palaeo-reticulated laterites of west Fujian. Some samples yielded unsatisfactory results, suggesting that the degree of bleaching of diluvial and alluvial deposits should be properly assessed before dating. We did not detect any enrichment/depletion of U, Th and radioactive disequilibrium. The effect of chemical weathering on the dose rate estimation was negligible. Therefore, we used a central age model and the maximum age model to calculate the age of two samples, respectively, and the minimum age model to calculate the ages of the rest of the samples. The OSL ages of the samples ranged from 27.09 ± 2.30 ka to 54.65 ± 7.39 ka for the 38–63 µm quartz size fraction, and roughly corresponded to the Marine Isotope Stage 3. In addition, three ages out of five are based on the calculation of minimum ages in this research, which needs to be further verified by other dating methods.
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References
Adamiec G, Aitken M, (1998) Dose-rate conversion factors: update. Ancient TL 16(2): 37–50.
Aitken MJ, (1998) An introduction to optical dating: the dating of Quaternary sediments by the use of photon-stimulated luminescence. Oxford University Press.
Andersen KK, Azuma N, Barnola JM, et al. (2004) High-resolution record of Northern Hemisphere climate extending into the last interglacial period. Nature 431(7005): 147–51. https://doi.org/10.1038/nature02805
Arnold LJ, Bailey RM, Tucker GE (2007) Statistical treatment of fluvial dose distributions from southern Colorado arroyo deposits. Quat Geochronol 2 (1–4): 162–167. https://doi.org/10.1016/j.quageo.2006.05.003
Arnold LJ, Demuro M, Ruiz MN (2012) Empirical insights into multi-grain averaging effects from ‘pseudo’ single-grain OSL measurements. Radiat Meas 47(9): 652–658. https://doi.org/10.1016/j.radmeas.2012.02.005
Bøtter-Jensen L, Andersen C, Duller G, et al. (2003) Developments in radiation, stimulation and observation facilities in luminescence measurements. Radiat Meas 37(4): 535–541. https://doi.org/10.1016/S1350-4487(03)00020-9
Brennan BJ, Lyons RG, Phillips SW (1991) Attenuation of alpha particle track dose for spherical grains. International Journal of Radiation Applications and Instrumentation. Part D. Nuclear Tracks and Radiat Meas 18(1): 249–253. https://doi.org/10.1016/1359-0189(91)90119-3
Duller GAT (2003) Distinguishing quartz and feldspar in single grain luminescence measurements. Radiat Meas 37(2): 161–165. https://doi.org/10.1016/S1350-4487(02)00170-1
Durcan JA, King GE, Duller GAT (2015) DRAC: Dose Rate and Age Calculator for trapped charge dating. Quat Geochronol 28: 54–61. https://doi.org/10.1016/j.quageo.2015.03.012
Fan X, Zhou Z, Wang X, et al. (2019) Brief report on the excavation of Longdengshan Paleolithic site in west of Fujian Province, China. Fujian Wenbo (3): 2–7. (In Chinese)
Fu X, Li SH (2013) A modified multi-elevated-temperature post-IR IRSL protocol for dating Holocene sediments using K-feldspar. Quat Geochronol 17: 44–54. https://doi.org/10.1016/j.quageo.2013.02.004
Galbraith RF, Roberts RG (2012) Statistical aspects of equivalent dose and error calculation and display in OSL dating: An overview and some recommendations. Quat Geochronol 11: 1–27. https://doi.org/10.1016/j.quageo.2012.04.020
Galbraith RF, Roberts RG, Laslett GM, et al. (1999) Optical dating of single and multiple grains of quartz from Jinmium Rock shelter, northern Australia: part 1, experimental design and statistical models. Archaeometry 41(2): 339–364. https://doi.org/10.1111/j.1475-4754.1999.tb00987.x
Gao L, Long H, Shen J, et al. (2017) Optical dating of Holocene tidal deposits from the southwestern coast of the South Yellow Sea using different grain-size quartz fractions. J Asian Earth Sci 135: 155–165. https://doi.org/10.1016/j.jseaes.2016.12.036
Guan Y, Gao X, Li F, et al. (2011) Modern human behaviors during the late stage of the MIS3 and the broad spectrum revolution: Evidence from a Shuidonggou Late Paleolithic site. Chin Sci Bull 57(4): 379–386. https://doi.org/10.1007/s11434-011-4828-x
Guérin G, Mercier N, Nathan R, et al. (2012) On the use of the infinite matrix assumption and associated concepts: A critical review. Radiat Meas 47(9): 778–785. https://doi.org/10.1016/j.radmeas.2012.04.004
Guo Y, Li B, Zhang J, et al. (2017) New ages for the Upper Palaeolithic site of Xibaimaying in the Nihewan Basin, northern China: implications for small-tool and microblade industries in north-east Asia during Marine Isotope Stages 2 and 3. J Quat Sci 32(4): 540–552. https://doi.org/10.1002/jqs.2949
Hu Y, Marwick B, Zhang J, et al. (2019) Late Middle Pleistocene Levallois stone-tool technology in southwest China. Nature 565(7737): 82–85. https://doi.org/10.1038/s41586-018-0710-1
Jacobs Z, Roberts RG, Lachlan TJ, et al. (2011) Development of the SAR TT-OSL procedure for dating Middle Pleistocene dune and shallow marine deposits along the southern Cape coast of South Africa. Quat Geochronol 6 (5): 491–513. https://doi.org/10.1016/j.quageo.2011.04.003
Jia L, Qiu Z (1960) The ages of strike stone in Gaungxi cave. Paleovertebrata et Paleoanthropologia 2(1): 64–68. (In Chinese)
Jin J, Li Z, Cheng Y, et al. (2018) Late Pleistocene aeolian activity in Haitan Island, Southeast China: Insights from optically stimulated luminescence dating of coastal dunes on marine terraces. J Mt Sci 15(8): 1777–1788. https://doi.org/10.1007/s11629-018-4890-9
Jin J, Li Z, Huang Y, et al. (2017) Chronology of a late Neolithic Age site near the southern coastal region of Fujian, China. Holocene 27(9): 1265–1272. https://doi.org/10.1177/0959683616687383
Lai Z, Mischke S, Madsen D (2013) Paleoenvironmental implications of new OSL dates on the formation of the “Shell Bar” in the Qaidam Basin, northeastern Qinghai-Tibetan Plateau. J Paleolimn 51(2): 197–210. https://doi.org/10.1007/s10933-013-9710-1
Lai Z, Zöller L, Fuchs M, et al. (2008) Alpha efficiency determination for OSL of quartz extracted from Chinese loess. Radiat Meas 43(2–6): 767–770. https://doi.org/10.1016/j.radmeas.2008.01.022
Li B, Li S-H (2011) Luminescence dating of K-feldspar from sediments: A protocol without anomalous fading correction. Quat Geochronol 6(5): 468–479. https://doi.org/10.1016/j.quageo.2011.05.001
Li S, Sun J, Zhao H (2002) Optical dating of dune sands in the northeastern deserts of China. Palaeogeogr Palaeoclimatol Palaeoecol 181(4): 419–429. https://doi.org/10.1016/s0031-0182(01)00443-6
Li Y (1982) On the relative age of the Paleolithic in Shouth China. Acta Anthropol Sin 1(2): 66–74. (In Chinese) CNKI:SUN:RLXB.0.1982-02-008
Li Z, Wu X, Zhou L, et al. (2017) Late Pleistocene archaic human crania from Xuchang, China. Science 355(6328): 969–972. https://doi.org/10.1126/science.aal2482
Meerbeeck CJV, Renssen H, Roche DM (2009) How did Marine Isotope Stage 3 and Last Glacial Maximum climates differ? — Perspectives from equilibrium simulations. Clim Past 5: 33–51. https://doi.org/10.5194/cp-5-33-2009
Murray AS, Wintle AG (2000) Luminescence dating of quartz using an improved single-aliquot regenerative-dose protocol. Radiat Meas 32(1): 57–73. https://doi.org/10.1016/S1350-4487(99)00253-X
Nian X, Chen F, Li F, et al. (2015) Optical dating of a Paleolithic site near the eastern coastal region of Shandong, northern China. Quat Geochronol 30: 466–471. https://doi.org/10.1016/j.quageo.2015.02.009
Nian X, Zhang W, Wang Z, et al. (2018) Optical dating of Holocene sediments from the Yangtze River (Changjiang) Delta, China. Quat Int 467: 251–263. https://doi.org/10.1016/j.quaint.2018.01.011
Olsen JW, Miller-Antonio S (1992) The Palaeolithic in Southern China. Asian Perspect 31(2): 129–160.
Pei W (1955) Chinese paleolithic culture. Science Press, Beijing. (In Chinese)
Smedley RK, Duller GAT, Rufer D, et al. (2020) Empirical assessment of beta dose heterogeneity in sediments: Implications for luminescence dating. Quat Geochronol 56: 101052. https://doi.org/10.1016/j.quageo.2020.101052
Sun Y, Clemens SC, Morrill C, et al. (2011) Influence of Atlantic meridional overturning circulation on the East Asian winter monsoon. Nature Geosci 5(1): 46–49. https://doi.org/10.1038/ngeo1326
Wang Y (1997) Pleistocene environment and the development of Paleolithic culture in southern China. Peking University Press, Beijing. (In Chinese)
Wang Y, Cheng H, Edwards RL, et al. (2008) Millennial- and orbital-scale changes in the East Asian monsoon over the past 224,000 years. Nature 451(7182): 1090–3. https://doi.org/10.1038/nature06692
Wang Y, Wang S (2014) New Achievements and Perspectives on Paleolithic Archaeology During the MIS3 Along the Eastern Foot of Songshan Mountain, Henan Province. Acta Anthropol Sin 33(3): 304–314. (In Chinese) CNKI:SUN:RLXB.0.2014-03-006
Zhang J, Li Y, Han Y, et al. (2019) Luminescence dating of weathered sediments from the Paleolithic site of Fengshuzui in northern Hunan province, China. Quat Geochronol 49: 211–217. https://doi.org/10.1016/j.quageo.2018.07.003
Zhang J, Nottebaum V, Tsukamoto S, et al. (2015) Late Pleistocene and Holocene loess sedimentation in central and western Qilian Shan (China) revealed by OSL dating. Quat Int 372: 120–129. https://doi.org/10.1016/j.quaint.2014.12.054
Zhang J, Yuan B, Zhou L (2008) Luminescence chronology of “Old Red Sand” in Jinjiang and its implications for optical dating of sediments in South China. Chinese Sci Bull 53(4): 591–601. https://doi.org/10.1007/s11434-008-0001-6
Zhang S (1983) On some problems of the upper Palaeolithic culture in Southern China. Acta Anthropol Sin 2(3): 218–230. CNKI:SUN:RLXB.0.1983-03-001
Zhang X, Zhu L, Huang Y, et al. (2020). The reticulated mechanism and its climatic implication of aggradation red earth. Quat Sci 40(1): 214–228. https://doi.org/10.11928/j.issn.1001-7410.2020.01.20
Riedesel S, Autzen M (2020) Dose-rate conversion function. Function version 0.1.0. In: Kreutzer S, Burow C, Dietze M, et al., Luminescence: Comprehensive Luminescence Dating Data Analysis. R package version 0.9.10.
Acknowledgments
This work was supported by National Natural Science Foundation of China (Grant Nos. 41301012, 42077407 and 41771020), Natural Science Foundation of Fujian Province, China (Grant No. 2020J01185), and the Innovation Research Team Fund of Fujian Normal University (Grant No. IRTL1705).
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Jin, Jh., Wang, Xy., Zhou, Zy. et al. OSL chronology of a Palaeolithic site in a humid subtropical mountainous area of southeast China. J. Mt. Sci. 18, 2012–2023 (2021). https://doi.org/10.1007/s11629-021-6701-y
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DOI: https://doi.org/10.1007/s11629-021-6701-y