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Inhibition of Heterogeneous Ice Nucleation by Bioinspired Coatings of Polyampholytes

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† †Key Laboratory of Green Printing, Institute of Chemistry and ‡Key Laboratory of Engineering Plastics, Institute of Chemistry, Chinese Academy of Sciences, Beijing 100190, China
§ University of Chinese Academy of Sciences, Beijing 100049, PR China
*E-mail: [email protected]
*E-mail: [email protected]
Cite this: ACS Appl. Mater. Interfaces 2017, 9, 35, 30092–30099
Publication Date (Web):August 16, 2017
https://doi.org/10.1021/acsami.7b10014
Copyright © 2017 American Chemical Society
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    Abstract

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    Control of heterogeneous ice nucleation (HIN) on foreign surfaces is of great importance for anti-ice-nucleation material design. In this work, we studied the HIN behaviors on various ion-modified poly(butylene succinate) (PBS) surfaces via chain-extension reaction. Inspired by antifreeze proteins (AFPs), the PBS-based polyampholytes, containing both negative and positive charge groups on a single chain, show excellent performance of ice nucleation inhibition and freezing delay. Unlike the extremely high price and low availability of AFPs, these PBS-based polyampholytes can be commercially synthesized under mild reaction conditions. Through water freezing tests on a wide range of substrates at different temperatures, these PBS-based polyampholytes have shown application value of tuning ice nucleation via a simple spin-coating method.

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    The Supporting Information is available free of charge on the ACS Publications website at DOI: 10.1021/acsami.7b10014.

    • 1H NMR spectrum of PBS-diol; experimental apparatus; melting behaviors, surface morphology, roughness, contact angle, and elemental analysis of PBS-based derivative surfaces; optical microscopic observation of freezing of a water droplet on PBS-based derivative surfaces (PDF)

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