On the design of single crystal diffractometers to measure a number of reflections simultaneously

Published under licence by IOP Publishing Ltd
, , Citation D C Phillips 1964 J. Sci. Instrum. 41 123 DOI 10.1088/0950-7671/41/3/302

0950-7671/41/3/123

Abstract

Single-crystal diffractometers derived from inclination Weissenberg goniometers can be adapted to measure more than one reflection at a time. Two reflections can be measured simultaneously, one from each of any two levels that are symmetrically on either side of the flat-cone setting, or several reflections can be measured quasi-simultaneously, one from each level within about ±0.05 r.l.u. of the flat-cone setting. The modifications which permit these new modes of operation are described, together with corresponding changes in the design and use of four-circle diffractometers. The general relationships between the two types of diffractometer are also discussed.

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10.1088/0950-7671/41/3/302