Review
In-situ Transmission Electron Microscope Techniques for Heterogeneous Catalysis
Bowen He,
Dr. Yixiao Zhang,
Prof. Xi Liu,
Prof. Liwei Chen,
Bowen He
In-situ Center for Physical Sciences School of Chemistry and Chemical Engineering, Shanghai Jiao Tong University, Shanghai, 200240 P.R. China
Search for more papers by this authorDr. Yixiao Zhang
In-situ Center for Physical Sciences School of Chemistry and Chemical Engineering, Shanghai Jiao Tong University, Shanghai, 200240 P.R. China
Search for more papers by this authorCorresponding Author
Prof. Xi Liu
In-situ Center for Physical Sciences School of Chemistry and Chemical Engineering, Shanghai Jiao Tong University, Shanghai, 200240 P.R. China
SynCat@Beijing, Synfuels China Technology Co.Ltd, Beijing, 101407 P.R. China
State Key Laboratory of Coal Conversion Institute of Coal Chemistry, Chinese Academy of Sciences, Taiyuan, 030001 P.R. China
Search for more papers by this authorCorresponding Author
Prof. Liwei Chen
In-situ Center for Physical Sciences School of Chemistry and Chemical Engineering, Shanghai Jiao Tong University, Shanghai, 200240 P.R. China
i-Lab, CAS Center for Excellence in Nanoscience Suzhou Institute of Nano-Tech and Nano-Bionics (SINANO), Chinese Academy of Sciences, Suzhou, 215123 P.R. China
Search for more papers by this author
Bowen He,
Dr. Yixiao Zhang,
Prof. Xi Liu,
Prof. Liwei Chen,
Bowen He
In-situ Center for Physical Sciences School of Chemistry and Chemical Engineering, Shanghai Jiao Tong University, Shanghai, 200240 P.R. China
Search for more papers by this authorDr. Yixiao Zhang
In-situ Center for Physical Sciences School of Chemistry and Chemical Engineering, Shanghai Jiao Tong University, Shanghai, 200240 P.R. China
Search for more papers by this authorCorresponding Author
Prof. Xi Liu
In-situ Center for Physical Sciences School of Chemistry and Chemical Engineering, Shanghai Jiao Tong University, Shanghai, 200240 P.R. China
SynCat@Beijing, Synfuels China Technology Co.Ltd, Beijing, 101407 P.R. China
State Key Laboratory of Coal Conversion Institute of Coal Chemistry, Chinese Academy of Sciences, Taiyuan, 030001 P.R. China
Search for more papers by this authorCorresponding Author
Prof. Liwei Chen
In-situ Center for Physical Sciences School of Chemistry and Chemical Engineering, Shanghai Jiao Tong University, Shanghai, 200240 P.R. China
i-Lab, CAS Center for Excellence in Nanoscience Suzhou Institute of Nano-Tech and Nano-Bionics (SINANO), Chinese Academy of Sciences, Suzhou, 215123 P.R. China
Search for more papers by this authorGraphical Abstract
Cooking with gas! Taking the gas-solid heterogeneous catalysis as an example, gas mixture can be introduced into the sample region of in-situ TEM during the imaging process. As a result, the kinetic surface evolution process of a catalyst can be monitored.
Abstract
The physicochemical properties of heterogeneous catalysts in static or inert environments often deviate greatly from the properties under in-situ or working conditions. To gain an insightful understanding of realistic catalyst properties and the corresponding catalytic mechanisms, it is essential to identify and rationalize changes in catalysts under reaction conditions. In recent years, in-situ transmission electron microscope (in-situ TEM) techniques have been increasingly developed, offering a unique approach to visualize the evolution of heterogeneous catalysis with ultra-high spatial resolution, good energy resolution and reasonable temporal resolution under controllable or even realistic catalytic conditions. In this review, we have summarized recent advances in the in-situ TEM analysis of heterogeneous catalysis, which suggests the great potential of this technique in this important field. Furthermore, technical challenges and possible solutions are discussed.
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