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Efficient Visible Light Degradation of Rhodamine B by a Photo-Electrochemical Process Based on a Bi2WO6 Nanoplate Film Electrode

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Key Laboratory of Pesticide and Chemical Biology of Ministry of Education, College of Chemistry, Central China Normal University, Wuhan 430079, People's Republic of China, and Department of Chemistry, Renmin University of China, Beijing 100872, People's Republic of China
Cite this: J. Phys. Chem. C 2007, 111, 18, 6832–6836
Publication Date (Web):April 13, 2007
https://doi.org/10.1021/jp070694z
Copyright © 2007 American Chemical Society
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    Abstract

    In this paper, a Bi2WO6 nanoplate film electrode was prepared by a hydrothermal method, combined with a spin coating technique. A photoelectrochemical (PEC) oxidation system based on this electrode was then constructed to degrade rhodamine B (RhB) in aqueous solution under visible light (λ > 420 nm). The PEC system based on Bi2WO6 nanoplate film electrode could degrade 87.2% of RhB with concentration of 5 mg/L in 120 min, operated at low voltage and under visible light irradiation, whereas only 36.8% and 39.5% degradation of RhB were observed for electro-oxidation process (EC) and photocatalytic oxidation process (PC), respectively, operated under the same condition. These results revealed a significant synergetic effect on degrading RhB via electro-oxidation and photocatalysis under visible light irradiation. A possible mechanism for this synergetic degradation of RhB was proposed on the basis of characterization results. Meanwhile, the degradation pathway of RhB during PEC under visible light irradiation was also discussed. This study provided an effective approach for aqueous organic pollutant removal by utilizing solar light.

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    †

     Central China Normal University.

    *

     Corresponding authors. E-mails:  L.Z., [email protected]; J.L., [email protected]. Tel/Fax:  +86-27-6786 7535.

    ‡

     Renmin University of China.

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    Nitrogen adsorption−desorption isotherms of the as-prepared Bi2WO6 powder, UV−vis absorbance spectra, plots of the (a)1/2 versus photon energy (hv) of the Bi2WO6 film on ITO, comparison of hydroxyl radical produced in the PC and PEC processes using tert-butyl alcohol as the chemical reagents, effect of applied bias potentials on the PEC process, and electrochemical impedance spectra of Bi2WO6/ITO electrode under different concentrations of RhB solution and different pH during PEC process. The material is available free of charge via the Internet at http://pubs.acs.org.

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